序号 | N (DMAEMA):n(氯化苄) | V (反应物):V(溶剂) | 时间/h | 温度/℃ | 产率/% |
1 | 1:2.5 | 1:2.5 | 5 | 20 | 82.93 |
2 | 1:2.5 | 1:2 | 10 | 25 | 82.12 |
3 | 1:2.5 | 1:1.5 | 15 | 30 | 79.54 |
4 | 1:2.5 | 1:1 | 20 | 35 | 92.10 |
5 | 1:2.5 | 1:0.5 | 25 | 40 | 82.46 |
6 | 1:2 | 1:2.5 | 10 | 30 | 83.86 |
7 | 1:2 | 1:2 | 15 | 35 | 77.59 |
8 | 1:2 | 1:1.5 | 20 | 40 | 90.56 |
9 | 1:2 | 1:1 | 25 | 20 | 81.21 |
10 | 1:2 | 1:0.5 | 5 | 25 | 73.89 |
11 | 1:1.5 | 1:2.5 | 15 | 40 | 78.96 |
12 | 1:1.5 | 1:2 | 20 | 20 | 72.02 |
13 | 1:1.5 | 1:1.5 | 25 | 25 | 83.28 |
14 | 1:1.5 | 1:1 | 5 | 30 | 74.51 |
15 | 1:1.5 | 1:0.5 | 10 | 35 | 79.90 |
16 | 1:1 | 1:2.5 | 20 | 25 | 64.33 |
17 | 1:1 | 1:2 | 25 | 30 | 83.15 |
18 | 1:1 | 1:1.5 | 5 | 35 | 79.45 |
19 | 1:1 | 1:1 | 10 | 40 | 83.73 |
20 | 1:1 | 1:0.5 | 15 | 20 | 77.73 |
21 | 1:0.5 | 1:2.5 | 25 | 35 | 70.65 |
22 | 1:0.5 | 1:2 | 5 | 40 | 81.20 |
23 | 1:0.5 | 1:1.5 | 10 | 20 | 72.29 |
24 | 1:0.5 | 1:1 | 15 | 25 | 73.40 |
25 | 1:0.5 | 1:0.5 | 20 | 30 | 76.36 |
均值1 | 83.8 | 76.1 | 78.4 | 77.2 |
|
均值2 | 81.4 | 79.2 | 79.4 | 75.4 |
|
均值3 | 77.7 | 81.0 | 77.4 | 79.5 |
|
均值4 | 77.7 | 80.9 | 79.1 | 79.9 |
|
均值5 | 74.8 | 77.5 | 80.2 | 82.4 |
|
极差 | 9.0 | 4.9 | 2.8 | 7.0 |
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