序号 | 温度(℃) | 溶剂b | 压强(MPa) | 转化率% | 产物% |
1 | 50 | DCM | 1 | 100 | 86.5 |
2 | 50 | DCE | 1 | 100 | 80.8 |
3 | 50 | CHCl3 | 1 | 100 | 79.6 |
4 | 50 | EA | 1 | 100 | 69.6 |
5 | 50 | THF | 1 | 100 | 19.0 |
6 | 50 | IPA | 1 | 100 | 0 |
7 | 15 | DCM | 1 | 100 | 79.3 |
8 | 25 | DCM | 1 | 100 | 80.3 |
9 | 35 | DCM | 1 | 100 | 82.7 |
10 | 45 | DCM | 1 | 100 | 83.4 |
11 | 55 | DCM | 1 | 100 | 83.5 |
12 | 50 | DCM | 2 | 100 | 86.5 |