Entry

Cat.

Solvent

t/h

Yieldb/%

1

None

H2O

12

-

2

MCM-41

H2O

12

-

3

PW

H2O

12

15

4

PM

H2O

12

10

5

20 wt% PW/MCM-41

H2O

12

25

6

50 wt% PW/MCM-41

H2O

12

36

7

60 wt% PW/MCM-41

H2O

12

36

8

70 wt% PW/MCM-41

H2O

12

29

9

80 wt% PW/MCM-41

H2O

12

30

10

50 wt% PM/MCM-41

H2O

12

25

11

50 wt% PW/MCM-41

CH2Cl2

12

10

12

50 wt% PW/MCM-41

CH3OH

12

trace

13

50 wt% PW/MCM-41

THF

12

79

14

50 wt% PW/MCM-41

Et2O

12

76

15

50 wt% PW/MCM-41

toluene

12

-

16

50 wt% PW/MCM-41

AcOEt

12

-

17 c

50 wt% PW/MCM-41

THF

12

82

18 d

50 wt% PW/MCM-41

THF

12

86

19

50 wt% PW/MCM-41

THF

6

56

20

50 wt% PW/MCM-41

THF

24

87