| 序号 | N (DMAEMA):n(氯化苄) | V (反应物):V(溶剂) | 时间/h | 温度/℃ | 产率/% |
| 1 | 1:2.5 | 1:2.5 | 5 | 20 | 82.93 |
| 2 | 1:2.5 | 1:2 | 10 | 25 | 82.12 |
| 3 | 1:2.5 | 1:1.5 | 15 | 30 | 79.54 |
| 4 | 1:2.5 | 1:1 | 20 | 35 | 92.10 |
| 5 | 1:2.5 | 1:0.5 | 25 | 40 | 82.46 |
| 6 | 1:2 | 1:2.5 | 10 | 30 | 83.86 |
| 7 | 1:2 | 1:2 | 15 | 35 | 77.59 |
| 8 | 1:2 | 1:1.5 | 20 | 40 | 90.56 |
| 9 | 1:2 | 1:1 | 25 | 20 | 81.21 |
| 10 | 1:2 | 1:0.5 | 5 | 25 | 73.89 |
| 11 | 1:1.5 | 1:2.5 | 15 | 40 | 78.96 |
| 12 | 1:1.5 | 1:2 | 20 | 20 | 72.02 |
| 13 | 1:1.5 | 1:1.5 | 25 | 25 | 83.28 |
| 14 | 1:1.5 | 1:1 | 5 | 30 | 74.51 |
| 15 | 1:1.5 | 1:0.5 | 10 | 35 | 79.90 |
| 16 | 1:1 | 1:2.5 | 20 | 25 | 64.33 |
| 17 | 1:1 | 1:2 | 25 | 30 | 83.15 |
| 18 | 1:1 | 1:1.5 | 5 | 35 | 79.45 |
| 19 | 1:1 | 1:1 | 10 | 40 | 83.73 |
| 20 | 1:1 | 1:0.5 | 15 | 20 | 77.73 |
| 21 | 1:0.5 | 1:2.5 | 25 | 35 | 70.65 |
| 22 | 1:0.5 | 1:2 | 5 | 40 | 81.20 |
| 23 | 1:0.5 | 1:1.5 | 10 | 20 | 72.29 |
| 24 | 1:0.5 | 1:1 | 15 | 25 | 73.40 |
| 25 | 1:0.5 | 1:0.5 | 20 | 30 | 76.36 |
| 均值1 | 83.8 | 76.1 | 78.4 | 77.2 |
|
| 均值2 | 81.4 | 79.2 | 79.4 | 75.4 |
|
| 均值3 | 77.7 | 81.0 | 77.4 | 79.5 |
|
| 均值4 | 77.7 | 80.9 | 79.1 | 79.9 |
|
| 均值5 | 74.8 | 77.5 | 80.2 | 82.4 |
|
| 极差 | 9.0 | 4.9 | 2.8 | 7.0 |
|