Entry
Br2 (eq.)
H2O (eq.)
m (Br2-H2O)/mg
T/℃
Yield/3a%b
Yield/4a%b
1
0.2
9.3
20
100
58
0
2
0.3
14
30
100
55
0
3
0.4
18.7
40
100
53
0
4
0.2
9.3
20
120
70
0
5
0.3
14
30
120
77
0
6
0.4
18.7
40
120
76
0
7
0.6
28
60
120
57
0
8
0.3
14
30
160
25
43
|
| ||||||
| Entry | Br2 (eq.) | H2O (eq.) | m (Br2-H2O)/mg | T/℃ | Yield/3a%b | Yield/4a%b |
| 1 | 0.2 | 9.3 | 20 | 100 | 58 | 0 |
| 2 | 0.3 | 14 | 30 | 100 | 55 | 0 |
| 3 | 0.4 | 18.7 | 40 | 100 | 53 | 0 |
| 4 | 0.2 | 9.3 | 20 | 120 | 70 | 0 |
| 5 | 0.3 | 14 | 30 | 120 | 77 | 0 |
| 6 | 0.4 | 18.7 | 40 | 120 | 76 | 0 |
| 7 | 0.6 | 28 | 60 | 120 | 57 | 0 |
| 8 | 0.3 | 14 | 30 | 160 | 25 | 43 |