Complex | 1 |
Empirical formula | C12H8N2O4Pb |
Formula weight | 451.39 |
Temperature | 293 (2) |
Crystal system | Orthorhombic |
Space group | P na21 |
a/Å | 26.264 (5) |
b/Å | 7.609 (5) |
c/Å | 5.832 (5) |
α/º | 90 |
β/º | 90 |
γ/º | 90 |
V/Å3 | 1165.5 (13) |
Z | 4 |
Dc/g cm−3 | 2.573 |
µ (Mo Kα)/mm−1 | 2.876 |
F (000) | 832 |
Reflections collected | 9168 |
Unique reflections | 2822 |
R (int) | 0.0459 |
GOF on F2 | 1.008 |
Final R indices [I>2sigma(I)] | R1 = 0.0402, wR2 = 0.0814 |
R indices (all data) | R1 = 0.0447, wR2 = 0.0826 |