Complex

1

Empirical formula

C12H8N2O4Pb

Formula weight

451.39

Temperature

293 (2)

Crystal system

Orthorhombic

Space group

P na21

a/Å

26.264 (5)

b/Å

7.609 (5)

c/Å

5.832 (5)

α/º

90

β/º

90

γ/º

90

V/Å3

1165.5 (13)

Z

4

Dc/g cm−3

2.573

µ (Mo Kα)/mm−1

2.876

F (000)

832

Reflections collected

9168

Unique reflections

2822

R (int)

0.0459

GOF on F2

1.008

Final R indices [I>2sigma(I)]

R1 = 0.0402, wR2 = 0.0814

R indices (all data)

R1 = 0.0447, wR2 = 0.0826