序号 | (1):(2):(3):(4):(5) (N) | 溶剂 | 温度(˚C) | 反应时间(h) | 平均产率(%) |
1 | 1:1.5:0.1:1:0.25 | 乙腈 | 80 | 2 | 45.6 |
2 | 1:1.5:0.2:1:0.25 | 68.3 | |||
3 | 1:1.5:0.3:1:0.25 | 86.6 | |||
4 | 1:1.5:0.4:1:0.25 | 66.7 | |||
5 | 1:1.5:0.5:1:0.25 | 61.4 | |||
6 | 1:1.5:0.3:0.25:0.25 | 58.9 | |||
7 | 1:1.5:0.3:0.5:0.25 |
|
|
| 63.7 |
8 | 1:1.5:0.3:0.75:0.25 |
|
|
| 78.4 |
9 | 1:1.5:0.3:1:0.25 |
|
|
| 86.6 |
10 | 1:1.5:0.3:1.25:0.25 |
|
|
| 80.6 |