3 | CH3OH | 1.5 | 6 | r.t | 86 |
4 | H2O | 1.5 | 12 | r.t | 67 |
5 | C2H5OH (95%) | 1.5 | 10 | r.t | 81 |
6 | C2H5OH | 1.5 | 5 | r.t | 80 |
7 | C2H5OH | 1.2 | 8 | r.t | 78 |
8 | C2H5OH | 1.0 | 12 | r.t | 76 |
9 | C2H5OH | 1.5 | 6 | 50 | 82 |
10 | C2H5OH | 1.5 | 7 | 80 | 80 |
11 | C2H5OH:H2O (1:1/v:v) | 1.5 | 9 | 50 | 73 |
12 | C2H5OH:H2O (2:1/v:v) | 1.5 | 7 | 50 | 78 |
13 | C2H5OH:H2O (3:1/v:v) | 1.5 | 6 | 50 | 85 |