Sample

Temperature of reduction Peaks (˚C)

Ratio of Co3+/(Co3+ + Co2+)

Ratio of Oads/(Oads + Olatt)

nanocloud Co3O4

306, 412

0.68

0.40

nanosphere Co3O4

297, 416

0.66

0.41

nanobook Co3O4

327, 440

0.68

0.43

nanoflower Co3O4

302, 381

0.64

0.40

nanorods Co3O4

369, 488

0.72

0.31