(1) A1B1C1 (36˚C, 50 rpm, 6 h)

(4) A2B1C2 (45˚C, 50 rpm, 8 h)

(7) A3B1C3(50˚C, 50 rpm, 10 h)

(2) A1B2C2 (36˚C, 100 rpm, 8 h)

(5) A2B2C3 (45˚C, 100 rpm, 10 h)

(8) A3B2C1(50˚C, 100 rpm, 6 h)

(3) A1B3C3 (36˚C, 150 rpm, 10 h)

(6) A2B3C1 (45˚C, 150 rpm, 6 h)

(9) A3B3C2(50˚C, 150 rpm, 8 h)