杂质 | 水平 | 本底量/mg | 加入量/mg | 测得量/mg | 回收率/% | 平均回收率/% | RSD/% |
氧化破坏杂质1 | 80% | 0 | 0.1618 | 0.1494 | 92.34 | 94.29 | 2.65 |
0 | 0.1618 | 0.1505 | 93.02 | ||||
0 | 0.1618 | 0.1498 | 92.58 | ||||
100% | 0 | 0.2023 | 0.1976 | 97.68 | |||
0 | 0.2023 | 0.1974 | 97.58 | ||||
0 | 0.2023 | 0.1974 | 97.58 | ||||
120% | 0 | 0.2427 | 0.2248 | 92.62 | |||
0 | 0.2427 | 0.2242 | 92.38 | ||||
0 | 0.2427 | 0.2254 | 92.87 | ||||
氧化破坏杂质2 | 80% | 0 | 0.1391 | 0.1363 | 97.99 | 96.35 | 1.64 |
0 | 0.1391 | 0.1363 | 97.99 | ||||
0 | 0.1391 | 0.1343 | 96.55 | ||||
100% | 0 | 0.1739 | 0.1702 | 97.87 | |||
0 | 0.1739 | 0.1688 | 97.07 | ||||
0 | 0.1739 | 0.1676 | 96.38 | ||||
120% | 0 | 0.2087 | 0.1982 | 94.97 | |||
0 | 0.2087 | 0.1970 | 94.39 | ||||
0 | 0.2087 | 0.1960 | 93.91 | ||||
Di-Gly2-生长抑素 | 80% | 0.008804 | 0.03075 | 0.04176 | 107.17 | 112.75 | 3.22 |
0.008792 | 0.03075 | 0.04248 | 109.55 | ||||
0.008784 | 0.03075 | 0.04288 | 110.88 | ||||
100% | 0.008788 | 0.03844 | 0.05146 | 111.01 | |||
0.008818 | 0.03844 | 0.05196 | 112.23 | ||||
0.008835 | 0.03844 | 0.05281 | 114.40 | ||||
120% | 0.008839 | 0.04613 | 0.06140 | 113.94 | |||
0.008830 | 0.04613 | 0.06274 | 116.87 | ||||
0.008864 | 0.04613 | 0.06364 | 118.74 | ||||
Des-Gly2-生长抑素 | 80% | 0.02010 | 0.1569 | 0.1733 | 97.64 | 99.16 | 1.23 |
0.02007 | 0.1569 | 0.1738 | 97.98 | ||||
0.02005 | 0.1569 | 0.1735 | 97.80 | ||||
100% | 0.02006 | 0.1962 | 0.2176 | 100.68 | |||
0.02012 | 0.1962 | 0.2174 | 100.55 | ||||
0.02016 | 0.1962 | 0.2175 | 100.58 | ||||
Des-Gly2-生长抑素 | 120% | 0.02017 | 0.2354 | 0.2530 | 98.91 |
|
|
0.02015 | 0.2354 | 0.2534 | 99.09 | ||||
0.02023 | 0.2354 | 0.2537 | 99.18 |