Entry

温度(℃)

1a用量(mmol)

投料比例1a:T:P

溶剂用量(mL)

2a收率(%)

2a纯度(%)

1

0~5

2

1:0.35:1.3

15

83.6

98.6

2

5~10

2

1:0.35:1.3

15

83.5

98.6

3

10~15

2

1:0.35:1.3

15

80.2

97.7

4

15~20

2

1:0.35:1.3

15

77.5

96.3

5

5~10

2

1:0.35:1.0

15

70.9

81.5

6

5~10

2

1:0.35:1.1

15

76.8

91.1

7

5~10

2

1:0.35:1.2

15

81.1

94.4

8

5~10

2

1:0.35:1.25

15

81.2

96.3

9

5~10

2

1:0.35:1.35

15

78.8

90.4

10

5~10

2

1:0.35:1.4

15

72.5

87.6

11

5~10

2

1:0.4:1.2

15

81.2

93.8

12

5~10

2

1:0.4:1.25

15

81.8

96.8

13

5~10

2

1:0.4:1.3

15

83.5

98.5